玻璃外层涂布均匀性控制机理及工艺优化研究进展

王砚鑫, 黄会轩, 李旭, 李艳, 袁英才, 任铮

包装工程(技术栏目) ›› 2026, Vol. 47 ›› Issue (19) : 247-259.

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包装工程(技术栏目) ›› 2026, Vol. 47 ›› Issue (19) : 247-259. DOI: 10.19554/j.cnki.1001-3563.2026.19.025
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玻璃外层涂布均匀性控制机理及工艺优化研究进展

  • 王砚鑫1, 黄会轩1, 李旭2, 李艳1, 袁英才1, 任铮1,*
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Research Progress on Mechanisms for Controlling Coating Uniformity on the Outer Layer of Glass and Process Optimization

  • WANG Yanxin1, HUANG Huixuan1, LI Xu2, LI Yan1, YUAN Yingcai1, REN Zheng1,*
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摘要

目的 系统梳理玻璃外层涂布均匀性形成机理,阐明典型缺陷的流体动力学本质并为工艺优化提供理论指导。方法 聚焦流涂、喷涂、浸涂、刮涂和狭缝涂布等5类典型外层涂布工艺,深入剖析涂料黏度、表面张力、屈服应力、固化行为及溶剂挥发等流变与物化特性对液膜稳定性的多尺度影响机制;系统总结了基于微观截面显微观测、非接触激光测厚、形貌三维重构、光学性能检测及胶带剥离等关键质量评价与缺陷表征方法;引入雷诺数(Re)、毛细数(Ca)、韦伯数(We)和邦德数(Bo)等关键流体力学无量纲数,探讨了基于多维精密涂布窗口理论的工艺参数协同优化策略。结果 研究发现,流挂主要受邦德数与毛细数共同控制,毛细脊形成与动态接触线迁移及表面张力梯度密切相关,空气卷入存在由毛细数主导的临界失稳条件;合理匹配涂料流变特性与工艺参数可有效拓宽稳定涂布窗口。结论 通过构建的“流变特性-动力学缺陷-工艺窗口”理论框架,可为大面积玻璃外层涂布的精准均匀性控制、多维界面缺陷抑制,以及高性能功能器件的高质量智能制造提供系统的理论参考与工程设计依据。

Abstract

The work aims to systematically review the mechanisms underlying the uniformity of outer-layer coating on glass, elucidate the fluid dynamic nature of typical defects, and provide theoretical guidance for process optimization. Focusing on five typical outer-layer coating processes, including flow coating, spray coating, dip coating, squeegee coating, and slot coating, the multiscale mechanisms by which rheological and physicochemical properties, such as coating viscosity, surface tension, yield stress, curing behavior, and solvent evaporation, affected liquid film stability were thoroughly analyzed; key quality evaluation and defect characterization methods, including microscopic observations of cross sections, non-contact laser thickness measurement, 3D morphological reconstruction, optical property testing, and tape peeling were systematically summarized; key fluid dynamics dimensionless numbers, such as the Reynolds number (Re), capillary number (Ca), Weber number (We), and Bond number (Bo) were introduced to explore strategies for the synergistic optimization of process parameters based on the theory of multidimensional precision coating windows. The study found that sagging was primarily controlled by the combined effects of the Bond number and the capillary number; capillary ridge formation was closely related to dynamic contact line migration and surface tension gradients; and air entrapment exhibited critical instability conditions dominated by the capillary number. Appropriately matching the rheological properties of the coating with process parameters could effectively broaden the stable coating window. The established "rheological properties, dynamic defects and process window" theoretical framework provides a systematic theoretical reference and engineering design basis for precise uniformity control in large-area glass outer-layer coating, suppression of multidimensional interfacial defects, and high-quality smart manufacturing of high-performance functional devices.

关键词

外层涂布 / 涂层均匀性 / 流变特性 / 涂布窗口 / 工艺优化

Key words

outer-layer coating / coating uniformity / rheological behavior / coating window / process optimization

引用本文

导出引用
王砚鑫, 黄会轩, 李旭, 李艳, 袁英才, 任铮. 玻璃外层涂布均匀性控制机理及工艺优化研究进展[J]. 包装工程. 2026, 47(19): 247-259 https://doi.org/10.19554/j.cnki.1001-3563.2026.19.025
WANG Yanxin, HUANG Huixuan, LI Xu, LI Yan, YUAN Yingcai, REN Zheng. Research Progress on Mechanisms for Controlling Coating Uniformity on the Outer Layer of Glass and Process Optimization[J]. Packaging Engineering. 2026, 47(19): 247-259 https://doi.org/10.19554/j.cnki.1001-3563.2026.19.025
中图分类号: TQ171    TB48   

参考文献

[1] KITTEL J, CELATI N, KEDDAM M, et al.Influence of the Coating-substrate Interactions on the Corrosion Protection: Characterisation by Impedance Spectroscopy of the Inner and Outer Parts of a Coating[J]. Progress in Organic Coatings, 2003, 46(2): 135-147.
[2] HAN X, YIN Z, PENG L, et al.A Scalable and Robust Synergistic Anti-icing and Anti-corrosion Bionic Dual-layer Coating Inspired by Peanut Seed Structure for Aircraft Wings[J]. Chemical Engineering Journal, 2026: 177322.
[3] SAHU N, PARIGA B, PANIGRAGI S.Fundamental Understanding and Modeling of Spin Coating Process: A Review[J]. Indian Journal of Physics, 2009, 83(4): 493-502.
[4] AKAFUAH N K, POOZESH S, SALAIMEH A, et al.Evolution of the Automotive Body Coating Process—A Review[J]. Coatings, 2016, 6(2): 24.
[5] FOTOVVATI B, NAMDRI N, DRHAHANGHADIKOLAEI A.On Coating Techniques for Surface Protection: A Review[J]. Journal of Manufacturing and Materials Processing, 2019, 3(1): 28.
[6] QUINTINO L.Overview of Coating Technologies[M]//Surface Modification by Solid State Processing. Woodhead Publishing, 2014: 1-24.
[7] MUSTAFA H A M, JAMEEL D A. Modeling and the Main Stages of Spin Coating Process: A Review[J]. Journal of Applied Science and Technology Trends, 2021, 2(02): 119-123.
[8] KARTHIKEYAN J.The Advantages and Disadvantages of the Cold Spray Coating Process[M]//The Cold Spray Materials Deposition Process. Woodhead Publishing, 2007: 62-71.
[9] SRIKANTH A, BASHA G M T, VENKATESHWARLU B. A Brief Review on Cold Spray Coating Process[J]. Materials Today: Proceedings, 2020, 22: 1390-1397.
[10] CHU H, XU N, YU X, et al.Review of Surface Modification in Pool Boiling Application: Coating Manufacturing Process and Heat Transfer Enhancement Mechanism[J]. Applied Thermal Engineering, 2022, 215: 119041.
[11] MEHMOOD A, ZUNAID M, MADAN A K.A Bibliometric Analysis of Cold Spray Coating Process Using VOSviewer[J]. Materials Today: Proceedings, 2022.
[12] FAN L, WANG F, WANG Z, et al.Study on the Influence of Surface Treatment Process on the Corrosion Resistance of Aluminum Alloy Profile Coating[J]. Materials, 2023, 16(17): 6027.
[13] BUTT M A.Thin-film Coating Methods: A Successful Marriage of High-quality and Cost-effectiveness—A Brief Exploration[J]. Coatings, 2022, 12(8): 1115.
[14] 王杰, 崔学军, 陈星佑, 等. 海泡石改性环氧树脂复合涂层的制备及其性能[J]. 中国表面工程, 2026, 39(1): 1-15.
WANG J, CUI X J, CHEN X Y, et al.Preparation and Properties of Sepiolite Modified Epoxy Resin Composite Coatings[J]. China Surface Engineering, 2026, 39(1): 1-15.
[15] 张钰, 陶冠羽, 曾路, 等. 氢能双极板涂层技术研究现状与发展[J]. 材料保护, 2026, 59(2): 1-34.
ZHANG Y, TAO G Y, ZENG L, et al.Research Status and Development of Coating Technology for Hydrogen Bipolar Plates[J]. Materials Protection, 2026, 59(2): 1-34.
[16] 樊彦峥, 潘永强, 刘金泽, 等. 热蒸发制备大口径铝膜的膜厚均匀性分析[J]. 光学与光电技术, 2021, 19(2): 108-114.
FAN Y Z, PAN Y Q, LIU J Z, et al.Thickness Uniformity Analysis of Large Aperture Aluminum Film Prepared by Thermal Evaporation[J]. Optics & Optoelectronic Technology, 2021, 19(2): 108-114.
[17] WAN T, STYLIOS G K.Effects of Coating Process on the Surface Roughness of Coated Fabrics[J]. The Journal of The Textile Institute, 2017, 108(5): 712-719.
[18] 葛伍群, 张惠庆, 张医军, 等. 流涂涂料及其工艺的研究[J]. 铸造, 1992(6): 13-16.
GE W Q, ZHANG H Q, ZHANG Y J, et al.Study on Flow Coating Materials and Its Technology[J]. Foundry, 1992(6): 13-16.
[19] 方世良. 树脂砂型流涂工艺质量控制[J]. 现代铸铁, 2015, 35(3): 66-70.
FANG S L.Quality Control of Flow Coating Process for Resin Sand Mold[J]. Modern Cast Iron, 2015, 35(3): 66-70.
[20] 聂爽, 王继东, 尹建伟, 等. 流涂工艺的常见问题及解决措施[J]. 铸造, 2012, 61(10): 1193-1196.
NIE S, WANG J D, YIN J W, et al.Common Problems and Solutions of Flow Coating Process[J]. Foundry, 2012, 61(10): 1193-1196.
[21] 王毅, 王国磊, 李波, 等. 大尺寸表面喷涂的交界区涂层均匀性分析[J]. 机械科学与技术, 2022, 41(11): 1705-1712.
WANG Y, WANG G L, LI B, et al.Analysis of Coating Uniformity in Boundary Zone of Large Size Surface Spraying[J]. Mechanical Science and Technology for Aerospace Engineering, 2022, 41(11): 1705-1712.
[22] 刘升明, 陈宗院, 张新娇, 等. 水性漆浸涂工艺探究[J]. 现代涂料与涂装, 2023, 26(12): 66-68.
LIU S M, CHEN Z Y, ZHANG X J, et al.Investigation on Dip Coating Process of Waterborne Paint[J]. Modern Coatings and Finishing, 2023, 26(12): 66-68.
[23] SUNG L P, JASMIN J, GU X, et al.Use of Laser Scanning Confocal Microscopy for Characterizing Changes in Film Thickness and Local Surface Morphology of UV-exposed Polymer Coatings[J]. Journal of Coatings Technology and Research, 2004, 1(4): 267-276.
[24] XIE Y, ZHAO T, LIU K.Characterization of Leveling and Sagging Effects on the Surface Quality of Coating Panels[J]. Surfaces and Interfaces, 2025, 62: 106215.
[25] PATRA K K, PANDA S.Formation of the Capillary Ridge on the Free Surface Dynamics of Second-grade Fluid over an Inclined Locally Heated Plate[J]. Zeitschrift für Naturforschung A, 2019, 74(12): 1099-1108.
[26] WANG X, BONACCURSO E, VENZMER J, et al.Deposition of Drops Containing Surfactants on Liquid Pools: Movement of the Contact Line, Marangoni Ridge, Capillary Waves and Interfacial Particles[J]. Colloids and Surfaces A: Physicochemical and Engineering Aspects, 2015, 486: 53-59.
[27] CHANG Y R, CHANG H M, LIN C F, et al.Three Minimum Wet Thickness Regions of Slot Die Coating[J]. Journal of Colloid and Interface Science, 2007, 308(1): 222-230.
[28] HALDER S, GRANDA R, WU J, et al.Air Bubble Entrapment During Drop Impact on Solid and Liquid Surfaces[J]. International Journal of Multiphase Flow, 2022, 149: 103974.
[29] FANG Z, YAN Y, LI C, et al.Bubble Defect Generation Mechanism in Slot Die Coating of High-viscosity Fluids[J]. ACS Applied Materials & Interfaces, 2024, 16(9): 11890-11900.
[30] LI M, HUANG K, YI X.Crack Formation Mechanisms and Control Methods of Laser Cladding Coatings: A Review[J]. Coatings, 2023, 13(6): 1117.
[31] SHEN X, HE X, GAO L, et al.Study on Crack Behavior of Laser Cladding Ceramic-metal Composite Coating with High Content of WC[J]. Ceramics International, 2022, 48(12): 17460-17470.
[32] CHAPPARD D, DEGASNE I, HURE G, et al.Image Analysis Measurements of Roughness by Texture and Fractal Analysis Correlate with Contact Profilometry[J]. Biomaterials, 2003, 24(8): 1-9.
[33] TAN P, DIAO S, HUANG T, et al.Numerical and Experimental Study on Coating Uniformity Control in Simultaneous Double-sided Slot Coating with a Novel Contacted Slot Die[J]. Chemical Engineering Science, 2020, 222: 115716.
[34] WHITESIDE P, CHININIS J, HUNT H.Techniques and Challenges for Characterizing Metal Thin Films with Applications in Photonics[J]. Coatings, 2016, 6(3): 35-60.
[35] OGLAKCI B, KUCUKYILDIRIM B, ÖZDUMAN Z, et al.The Effect of Different Polishing Systems on the Surface Roughness of Nanocomposites: Contact Profilometry and SEM Analyses[J]. Operative Dentistry, 2021, 46(2): 173-187.
[36] VAN ZELE M, WATTÉ J, HASSELMEYER J, et al.Thickness Characterization Toolbox for Transparent Protective Coatings on Polymer Substrates[J]. Materials, 2018, 11(7): 1101.
[37] SUN H, SONG B, SUN X, et al.Recent Representative Progress of Surface Coating Technology[J]. The Chemical Record, 2025, 25(8): e202500054.
[38] DOLGOV M A.Analysis of the Stress State in the Deformed Coating Under Base Stretching with the Bending Effect Account[J]. Strength of Materials, 2024, 56(6): 1127-1135.
[39] PARK K, CHOE S, SADEGHI K, et al.Effect of Epichlorohydrin Treatment on the Coating Process and Performance of High-barrier Paper Packaging[J]. Food Chemistry, 2024, 445: 138772.
[40] MERSAGH DEZFULI S, SABZI M.Deposition of Ceramic Nanocomposite Coatings by Electroplating Process: A Review of Layer-deposition Mechanisms and Effective Parameters on the Formation of the Coating[J]. Ceramics International, 2019, 45(17): 21835-21842.
[41] CHEN C, WEI M, GUO X, et al.Effects of Welding Parameters on Inconel 625 Coating Synthesised by Tungsten Inert Gas Cladding[J]. Materials Science and Technology, 2024, 40(9): 701-712.
[42] LUBIS S, SIREGAR M A, DAMANIK W S, et al.Flow Numerical Analysis in the Process of Pouring Resin on Pelton Turbine Blade Molds Using Solidworks Software[C]//International Conference on Research Innovations: Trends in Science and Technology. Penang, Malaysia, 2023: 040002.
[43] SIROTA V V, SAVOTCHENKO S E, STROKOVA V V, et al.Control over Technological Parameters of Detonation Spraying for Producing Titanium Dioxide Coatings with Specified Wetting Properties[J]. Colloid Journal, 2024, 86(5): 781-790.
[44] ŁUCARZ M, DROŻYŃSKI D, KACZMARSKA K, et al. Influence of the Applied Protective Coating on the Technological Parameters of the Moulding or Core Sand Surface[J]. Materials, 2024, 17(23): 5737.
[45] SPIEGEL S, HOFFMANN A, KLEMENSL J, et al.High-speed Slot-die Coating of Primer Layers for Li-ion Battery Electroces: Model Calculations and Experimental Validation of the Extended Coating Window Depending on Coating Speed, Coating Gap and Viscosity[J]. Journal of Coatings Technology and Research, 2024, 21(2): 493-505.
[46] LEE S H, KOH H J, RYU B K, et al.Operability Coating Windows and Frequency Response in Slot Coating Flows from a Viscocapillary Model[J]. Chemical Engineering Science, 2011, 66(21): 4953-4959.
[47] HAN S K, SHIN D M, PARK H Y, et al.Effect of Viscoelasticity on Dynamics and Stability in Roll Coatings[J]. The European Physical Journal Special Topics, 2009, 166(1): 107-110.
[48] JI H S, AHN W G, KWON I, et al.Operability Coating Window of Dual-layer Slot Coating Process Using Viscocapillary Model[J]. Chemical Engineering Science, 2016, 143: 122-129.
[49] SCHMITT M, BAUNACH M, WENGELER L, et al.Slot-die Processing of Lithium-ion Battery Electrodes—Coating Window Characterization[J]. Chemical Engineering and Processing: Process Intensification, 2013, 68: 32-37.
[50] CHIN C P, WU H S, WANG S S.Improved Coating Window for Slot Coating[J]. Industrial & Engineering Chemistry Research, 2010, 49(8): 3802-3809.
[51] PATIDAR R, BURKITT D, HOOPER K, et al.Slot-die Coating of Perovskite Solar Cells: An Overview[J]. Materials Today Communications, 2020, 22: 100808.
[52] KARAOGLAN A D, OZDEN E.Electrostatic Powder Coating Process Optimisation by Implementing Design of Experiments[J]. Transactions of the IMF, 2021, 99(1): 46-52.
[53] DING X, LIU Y, et al.A Review of the Operating Limits in Slot Die Coating Processes[J]. AICHE Journal, 2016, 62(7): 2508-2524.

基金

2025年国家级大学生创新创业训练计划项目-基于肌腱驱动机构的自适应软夹持器设计(202510015011); 机械专业学位博士点申报建设(21090126006); 数字化印刷装备北京市重点实验室建设项目(KYCPT202508); 智能与绿色柔版印刷重点实验室2024年度招标课题(ZBKT202402)

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