Determination of Cr(VI) Residues in Paper-made Packaging by Continuous Flow Method after Solid Phase Extraction Cleanup

WANG Hong-bo, ZHAO Le, GUO Jun-wei, ZHU Xian-yue, YIN Yan-qi, XIE Yu-long, LIU Hui-min

Packaging Engineering ›› 2016 ›› Issue (1) : 107-110163.

Packaging Engineering ›› 2016 ›› Issue (1) : 107-110163.

Determination of Cr(VI) Residues in Paper-made Packaging by Continuous Flow Method after Solid Phase Extraction Cleanup

  • WANG Hong-bo1, ZHAO Le1, GUO Jun-wei1, LIU Hui-min1, ZHU Xian-yue2, XIE Yu-long2, YIN Yan-qi3
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Abstract

The aim of this study was to develop a method for the determination of Cr(VI) residues in paper-made packaging by continuous flow method after solid phase extraction cleanup. Cr(VI) was extracted from the sample by oscillation using the solution of potassium hydrogen phosphate (pH=8.0), cleaned up by solid phase extraction of polyamide, and then determined by continuous flow method. The detection limit of Cr(VI) in the method was 0.044 mg/kg, the recovery was in the range of 84.0%~99.0%, and the relative standard deviation (RSD) was less than 8.60%. The real sample analysis showed that this simple, fast and accurate method could be used for the determination of the residues of Cr(VI) in paper-made packaging samples.

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WANG Hong-bo, ZHAO Le, GUO Jun-wei, ZHU Xian-yue, YIN Yan-qi, XIE Yu-long, LIU Hui-min. Determination of Cr(VI) Residues in Paper-made Packaging by Continuous Flow Method after Solid Phase Extraction Cleanup[J]. Packaging Engineering. 2016(1): 107-110163

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