发射箱用RTM树脂体系工艺性与固化性能研究

徐淑权, 黄立果, 蔡建, 秦旭锋, 白焘, 汪道全

包装工程(技术栏目) ›› 2016 ›› Issue (1) : 115-119.

包装工程(技术栏目) ›› 2016 ›› Issue (1) : 115-119.

发射箱用RTM树脂体系工艺性与固化性能研究

  • 徐淑权1, 蔡建1, 秦旭锋1, 白焘1, 汪道全1, 黄立果2
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Process and Curing Properties of RTM Resin System for Launch Box

  • XU Shu-quan1, CAI Jian1, QIN Xu-feng1, BAI Tao1, WANG Dao-quan1, HUANG Li-guo2
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摘要

目的 研究环氧树脂体系的黏度及固化性能, 为利用树脂传递模塑(RTM)工艺制造发射箱提供理论依据。方法 采用旋转黏度计测试了E-51环氧树脂体系的动态黏度和静态黏度, 用非等温DSC法和平板小刀法研究了树脂体系的固化行为。结果 在60~80 ℃下70 min, 树脂体系的黏度仍小于1000 mPa·s, 符合工艺要求, 并推导出了固化温度参数分别为60, 125, 180 ℃, 以及凝胶时间与温度的关系方程。结论 温度区间60~80 ℃可作为发射箱RTM工艺的操作区间, 建议固化工艺制度为60,90, 125 ℃下分别加热固化3.5, 2, 1 h, 后处理工艺为180 ℃下加热固化1 h。

Abstract

The aim of this work was to study the viscosity and curing properties of epoxy resin system, in order to provide a theoretical basis for manufacturing launch box using RTM process. The dynamic viscosity and static viscosity of the E-51epoxy resin system were tested by rotational viscometer. The curing behavior of the resin system was studied using the non-isothermal DSC method and Flat knife method. The viscosity of the resin system was still less than 1000 mPa·s after 70 min at 60~80 ℃, which met the process requirements. And it was deduced that the curing temperature parameter was 60, 125 and 180 ℃ respectively, as well as the relationship equation of gel time and temperature. The temperature range 60~80 ℃ could be used as the operating range for RTM process to manufacture launch box. The recommended curing process of system was heat curing 3.5, 2 and 1 h at 60,90 and 125 ℃respectively, post-treatment process for the next 1h at 180 ℃.

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徐淑权, 黄立果, 蔡建, 秦旭锋, 白焘, 汪道全. 发射箱用RTM树脂体系工艺性与固化性能研究[J]. 包装工程(技术栏目). 2016(1): 115-119
XU Shu-quan, HUANG Li-guo, CAI Jian, QIN Xu-feng, BAI Tao, WANG Dao-quan. Process and Curing Properties of RTM Resin System for Launch Box[J]. Packaging Engineering. 2016(1): 115-119

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