食品容器中双酚A的一种现场检测方法

罗敏, 张吉坪, 李晨曦, 周冕

包装工程(技术栏目) ›› 2014 ›› Issue (15) : 11-14.

包装工程(技术栏目) ›› 2014 ›› Issue (15) : 11-14.

食品容器中双酚A的一种现场检测方法

  • 罗敏1, 张吉坪1, 李晨曦1, 周冕2
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A Portable Method for Rapid Determination of Bisphenol A in Food Containers

  • LUO Min1, ZHANG Ji-ping1, LI Chen-xi1, ZHOU Mian2
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摘要

目的 鉴于实验室仪器分析方法不适合现场快速检测食品容器中的双酚A,建立薄层色谱(TLC)方法对样品中双酚 A 进行定性检测。 方法 以 PC 材质桶装水水桶作为样品, 甲醇为提取溶剂 , 石油醚/乙酸乙酯/乙腈体系(体积比为 7∶3∶0.5)为展开剂 , 碘蒸汽显色, 检测出食品容器中的双酚A, 并通过红外光谱验证测定结果。 结果 采用 TLC 法能有效地分离检测食品容器中的双酚A。 结论 TLC 法操作简便、灵敏度高、重现性好,适用于食品容器中双酚A的现场快速检测。

Abstract

Objective To set up a thin layer chromatography (TLC) assay for qualitative determination of bisphenol A in food containers as a field rapid determination method to overcome the disadvantages of laboratory instrumental analysis. Methods Bisphenol A was determined by extracting from polycarbonate (PC) water bottle with methanol, eluting with petroleum ether/ethyl acetate/acetonitrile (volume ratio 7∶3∶0.5) and developing color with iodine steam on TLC plate. And the determination results were further verified by infrared spectroscopy. Results Bisphenol A in food containers was effectively detected by TLC. Conclusion This method is convenient, sensitive and highly reproducible, and is therefore suitable for rapid field determination of bisphenol A in food containers.

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导出引用
罗敏, 张吉坪, 李晨曦, 周冕. 食品容器中双酚A的一种现场检测方法[J]. 包装工程(技术栏目). 2014(15): 11-14
LUO Min, ZHANG Ji-ping, LI Chen-xi, ZHOU Mian. A Portable Method for Rapid Determination of Bisphenol A in Food Containers[J]. Packaging Engineering. 2014(15): 11-14

基金

重庆理工大学拔尖创新人才培养项目(BC201204)

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