建立了加速溶剂萃取-气相相色谱-串联质谱法测定食品接触材料（婴儿奶瓶）中双酚A、双酚F及其衍生物残留量的分析方法。样品用二氯甲烷作提取剂，用加速溶剂萃取仪进行了提取，经乙酸酐衍生化，用气相色谱-串联质谱仪进行了定性、定量分析。结果表明：BPA,BPF, BADGE,BFDG 4种化合物的回收率范围在78.9%～101.1%之间，相对标准偏差小于10%，线性关系良好，方法的检出限分别为0.2，0.1，5，5 ng/g，该方法简便、快速、灵敏度高、重复性好。

An accelerated solvent extraction followed by gas chromatography-tandem mass spectrometry was developed for determination of bisphenol A, bisphenol F and their derivatives residuals in food contact materials. Samples were extracted with dichloromethane in an accelerated solvent extractor, and derivatized by a commercial acetic anhydride prior to GC-MS/MS analysis. The results showed that the recovery of BPA, BPF, BFDGE and BADGE was in the range of 78.9%～101.1%, with the relative standard deviation (RSD) value less than 10%; the linearity is good (R-2 > 0.995); the detection limits are 0.2, 0.1, 5, and 5 ng/g respectively. It was concluded that the method is simple, fast, sensitive, and of good repeatability.