锐孔-凝固浴法制备米邦塔仙人掌多酚微胶囊的研究

赵永康; 王铄; 杜贝尔; 马心怡; 王鑫; 赛娜

doi:10.19554/j.cnki.1001-3563.2026.13.023

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包装工程（技术栏目） ›› 2026, Vol. 47 ›› Issue (13) : 201-214. DOI: 10.19554/j.cnki.1001-3563.2026.13.023

农产品保鲜与食品包装

锐孔-凝固浴法制备米邦塔仙人掌多酚微胶囊的研究

赵永康¹, 王铄¹, 杜贝尔¹, 马心怡¹, 王鑫^1,2*, 赛娜³

作者信息 +

Preparation of Microcapsules Containing Polyphenols from Opuntia ficus-indica with the Pore-solidification Bath Method

ZHAO Yongkang¹, WANG Shuo¹, DU Beier¹, MA Xinyi¹, WANG Xin^1,2*, SAI Na³

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文章历史 +

摘要

目的选取米邦塔仙人掌多酚作为芯材,制备一种以壳聚糖/海藻酸钠为复合壁材的具有缓释、抗氧化功能的微胶囊,为开发新型智能食品包装材料提供理论依据与技术支撑。方法采用低共熔溶剂（DES）提取米邦塔仙人掌多酚,以包埋率和产率为指标,通过单因素结合响应面实验确定微胶囊最优制备工艺,按此工艺制备微胶囊,并对其进行初步的性能评价。结果微胶囊制备最佳工艺条件如下：芯壁比为1∶2、包埋时间为1.5 h、海藻酸钠质量分数为2.7%。在该条件下,微胶囊包封率达(92.5±2.98)%、产率达(60.02±3.64)%,平均粒径为(359.22±6.6) μm。红外光谱分析显示,相较于多酚纯品,在1 051 cm^-1处,微胶囊中多酚特征吸收峰减弱且无新峰出现。体外模拟胃肠释放实验表明,该微胶囊具有良好的缓释性能,多酚释放平稳。米邦塔仙人掌微胶囊DPPH·自由基清除率最高达60.0%,ABTS⁺自由基清除率最高为80.10%。结论成功制备了一种具有缓释性及抗氧化性的微胶囊,为米邦塔多酚的绿色提取、稳定递送提供了技术支撑与理论参考。其优异的抗氧化性能亦表明其作为天然抗氧化剂在延长食品货架期及活性包装涂层中具有广阔的应用前景。

Abstract

The work aims to prepare microcapsules with sustained-release and antioxidant properties by taking polyphenols from Opuntia ficus-indica as the core material and chitosan/sodium alginate composites as the shell material, providing a theoretical basis and technical support for the development of novel smart food packaging materials. Polyphenols were extracted from Opuntia ficus-indica with a deep eutectic solvent (DES). The optimal microcapsule preparation process was determined through single-factor and response surface experiments, with encapsulation efficiency and yield as indicators. Microcapsules were prepared according to this process and subjected to preliminary performance evaluation. The optimal microcapsule preparation conditions were determined to be a core-to-shell ratio of 1:2, an encapsulation time of 1.5 h, and a sodium alginate mass fraction of 2.7%. Under these conditions, the encapsulation efficiency reached (92.5±2.98)%, the yield reached (60.02±3.64)%, and the average particle size was approximately (359.22±6.6) μm. Infrared spectroscopic analysis showed that, compared to the pure polyphenol, the characteristic absorption peak of polyphenols at 1 051 cm^-1 was weakened in the microcapsules, and no new peaks appeared. In vitro simulated gastrointestinal release experiments indicated that the microcapsules exhibited good sustained-release properties, with a steady release of polyphenols. The DPPH radical scavenging rate of the Opuntia ficus-indica microcapsules reached up to 60.0%, and the ABTS⁺ radical scavenging rate reached up to 80.10%. The microcapsules with sustained-release and antioxidant properties are successfully prepared, providing technical support and theoretical guidance for the green extraction and stable delivery of Opuntia ficus-indica polyphenols. Their excellent antioxidant properties also indicate that they hold broad application prospects as natural antioxidants in extending food shelf life and in active packaging coatings.

导出引用

赵永康, 王铄, 杜贝尔, 马心怡, 王鑫, 赛娜. 锐孔-凝固浴法制备米邦塔仙人掌多酚微胶囊的研究[J]. 包装工程. 2026, 47(13): 201-214 https://doi.org/10.19554/j.cnki.1001-3563.2026.13.023

ZHAO Yongkang, WANG Shuo, DU Beier, MA Xinyi, WANG Xin, SAI Na. Preparation of Microcapsules Containing Polyphenols from Opuntia ficus-indica with the Pore-solidification Bath Method[J]. Packaging Engineering. 2026, 47(13): 201-214 https://doi.org/10.19554/j.cnki.1001-3563.2026.13.023

中图分类号： TB34

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