纳米SiO2改性生物降解复合薄膜研究

陈志周, 牟建楼, 刘玮佳, 于志彬, 孙兰芳

包装工程(技术栏目) ›› 2019 ›› Issue (3) : 86-93.

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包装工程(技术栏目) ›› 2019 ›› Issue (3) : 86-93. DOI: 10.19554/j.cnki.1001-3563.2019.03.012

纳米SiO2改性生物降解复合薄膜研究

  • 陈志周, 牟建楼, 刘玮佳, 于志彬, 孙兰芳
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Nano SiO2 Modified Biodegradable Composite Films

  • CHEN Zhi-zhou, MOU Jian-lou, LIU Wei-jia, YU Zhi-bin, SUN Lan-fang
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摘要

目的 以壳聚糖(chitosan)、木薯淀粉和聚乙烯醇(PVA)为基础成膜原料,探究纳米SiO2改性木薯淀粉/PVA/壳聚糖薄膜的制备工艺过程。方法 以薄膜断裂伸长率、抗张强度、透光率和吸水率为评判标准,在单因子试验基础上,设计L9(34)正交试验,研究纳米SiO2含量、分散剂十二烷基苯磺酸含量、膜液pH值等3个因素对纳米SiO2改性木薯淀粉/聚乙烯醇/壳聚糖薄膜性能的影响。结果 得出了制备纳米SiO2改性木薯淀粉/PVA/壳聚糖薄膜的最佳工艺参数,纳米SiO2质量分数为2.0%、十二烷基苯磺酸钠质量分数为2.0%、膜液pH值为3.0,3个因素对改性薄膜性能的影响程度大小排序为分散剂含量>纳米SiO2含量>pH值。结论 获得了纳米SiO2改性木薯淀粉/PVA/壳聚糖薄膜的最佳生产工艺参数。

Abstract

The work aims to study the preparation technology process of Nano-SiO2 modified cassava starch/ PVA/chitosan film, with chitosan, cassava starch and polyvinyl alcohol (PVA) as basic film-forming materials. With elongation at break, tensile strength, transmittance and water absorption as evaluation index, based on single factor test, the influences of the Nano-SiO2 content, the content of dispersant SDBS and the pH value of casing solution on properties of Nano-SiO2 modified cassava starch/PVA/chitosan films were studied through the design of L9 (34) orthogonal experiment. The best process parameters for the preparation of Nano-SiO2 modified cassava starch/PVA/chitosan film were obtained. The mass fraction of Nano-SiO2 was 2.0%, the mass fraction of SDBS was 2.0%, and the pH value of casting solution was 3.0. The ranking of three factors affecting the modified film performance was dispersant content>Nano-SiO2 content>pH value. The best production process parameters of Nano-SiO2 modified cassava starch/PVA/chitosan films are obtained.

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陈志周, 牟建楼, 刘玮佳, 于志彬, 孙兰芳. 纳米SiO2改性生物降解复合薄膜研究[J]. 包装工程(技术栏目). 2019(3): 86-93 https://doi.org/10.19554/j.cnki.1001-3563.2019.03.012
CHEN Zhi-zhou, MOU Jian-lou, LIU Wei-jia, YU Zhi-bin, SUN Lan-fang. Nano SiO2 Modified Biodegradable Composite Films[J]. Packaging Engineering. 2019(3): 86-93 https://doi.org/10.19554/j.cnki.1001-3563.2019.03.012

基金

河北省科技计划(17227117D);河北省食品科学与工程学科“双一流”建设资金项目(2016SPGCA18)

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