响应面法优化制备壳聚糖明胶活性膜

白旭, 王愈, 王宝刚, 李文生, 杨田田

包装工程(技术栏目) ›› 2018 ›› Issue (9) : 24-30.

PDF(2308 KB)
PDF(2308 KB)
包装工程(技术栏目) ›› 2018 ›› Issue (9) : 24-30. DOI: 10.19554/j.cnki.1001-3563.2018.09.005

响应面法优化制备壳聚糖明胶活性膜

  • 白旭1, 王愈2, 王宝刚3, 李文生4, 杨田田4
作者信息 +

Optimization and Preparation of Chitosan/gelatin-based Active Films in Response Surface Methodology

  • BAI Xu1, WANG Yu2, WANG Bao-gang3, LI Wen-sheng4, YANG Tian-tian4
Author information +
文章历史 +

摘要

目的 制备一种具有疏水功能的壳聚糖-明胶活性膜。方法 通过研究不同质量浓度比的明胶-壳聚糖对膜性能的影响,确定两者的最佳质量浓度比,并研究柠檬酸三丁酯、甘油、吐温-20浓度对活性膜疏水性能的影响。根据Box-Benhnken试验设计原理,以膜的抗拉强度作为响应值,对活性疏水膜的制备工艺进行优化。探讨各因素交互作用,确定制备壳聚糖-明胶活性疏水膜的最佳条件。结果 明胶-壳聚糖的最佳质量浓度比为1∶1,各因素对膜抗拉强度的显著性影响依次是柠檬酸三丁酯>甘油>吐温-20。经过验证,制备活性膜时,柠檬酸三丁酯、甘油、吐温-20的最佳质量浓度分别为0.9,0.3,0.1 g/mL,该条件下膜的抗拉强度为20.9 MPa,断裂伸长率为41.34%。结论 该工艺条件下所制备的活性膜感官性能、物理性能和疏水性能均良好。

Abstract

The work aims to prepare chitosan/gelatin active films with hydrophobic function. The effects of gelatin-chitosan with different mass concentrations ratios on the film properties were studied to determine the best mass concentrations ratio of the two. The effect of tributyl citrate, glycerol and Tween-20 concentration on the hydrophobic properties of the active films was also studied. The preparation technology of active hydrophobic films was optimized based on the design principle of Box-Benhnken test, with tensile strength of the film as the response value. The interaction of various factors was explored to determine the optimum conditions for the preparation of chitosan-gelatin active films. The best mass concentrations ratio of gelatin/chitosan was 1∶1. The significant effect of three factors on tensile strength of films successively followed by tributyl citrate > glycerol > Tween-20. After verification, during the preparation of active films, the best mass concentrations of tributyl citrate, glycerol and Tween-20 were respectively 0.9, 0.3 and 0.1g/mL. Under this condition, the tensile strength of film was 20.9 MPa, and the elongation at break was 41.34%. The sensory, physical and hydrophobic properties of the active films prepared under this process are favorable.

引用本文

导出引用
白旭, 王愈, 王宝刚, 李文生, 杨田田. 响应面法优化制备壳聚糖明胶活性膜[J]. 包装工程(技术栏目). 2018(9): 24-30 https://doi.org/10.19554/j.cnki.1001-3563.2018.09.005
BAI Xu, WANG Yu, WANG Bao-gang, LI Wen-sheng, YANG Tian-tian. Optimization and Preparation of Chitosan/gelatin-based Active Films in Response Surface Methodology[J]. Packaging Engineering. 2018(9): 24-30 https://doi.org/10.19554/j.cnki.1001-3563.2018.09.005

基金

北京市农林科学院青年基金(QNJJ201709);北京市农林科学院科技创新能力建设专项(KJCX20170206)

PDF(2308 KB)

Accesses

Citation

Detail

段落导航
相关文章

/